INSTRUMENT CONTROL PARAMETERS:    5973 MSD LS-106
                           -------------------------------------------------

   C:\MSDCHEM\1\METHODS\TENAX+TDS_noquickswapB.M

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  Manual
Injection Location:  Front
Mass Spectrometer :  Enabled

=============================================================================
                                6890 GC METHOD
=============================================================================


OVEN
   Initial temp:  30 'C (On)               Maximum temp:  255 'C
   Initial time:  3.00 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time   CRYO (N2)
      1  7.00      110        0.00         Cryo:  Off
      2  5.00      250       10.00         Cryo fault:  On
      3   0.0(Off)                         Cryo timeout:  20.00 min (On)
   Post temp:  30 'C                       Quick cryo cool:  Off
   Post time:  0.00 min                    Ambient temp:  25 'C
   Run time:  52.43 min


FRONT INLET (CIS3)                      BACK INLET (UNKNOWN)
   Mode:  Solvent Vent
   Initial temp:  250 'C (Off)
   Pressure:  7.97 psi (On)
   Vent time:  0.10 min
   Vent flow:  30.0 mL/min
   Vent Pressure:  8.0 psi
   Purge flow:  30.0 mL/min
   Purge time:  1.00 min
   Total flow:  34.3 mL/min
   Gas saver:  Off
   Gas type:  Helium


COLUMN 1                                COLUMN 2
   Capillary Column                        (not installed)
   Model Number:  Restek 12424
   Rtx-Wax
   Max temperature:  250 'C
   Nominal length:  30.0 m
   Nominal diameter:  320.00 um
   Nominal film thickness:  0.25 um
   Mode:  constant flow
   Initial flow:  1.6 mL/min
   Nominal init pressure:  7.97 psi
   Average velocity:  26 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  1.00 psi


FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)


SIGNAL 1                                SIGNAL 2
   Data rate:  5 Hz                        Data rate:  20 Hz
   Type:  aux #5   pressure                Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0


COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)


THERMAL AUX 2                           AUX PRESSURE 3
   Use:  MSD Transfer Line Heater          Description:  HS syringe purge
   Description:  Transfer Line             Gas Type:  Helium
   Initial temp:  280 'C (On)              Initial pressure:  7.25 psi (On)
   Initial time:  0.00 min                 Initial time:  0.00 min
      #  Rate  Final temp  Final time         #  Rate  Final pres  Final time
      1   0.0(Off)                            1   0.0(Off)


AUX PRESSURE 4                          AUX PRESSURE 5
   Description:                            Description:  Ouick Swap
   Gas Type:  Helium                       Gas Type:  Helium
   Initial pressure:  0.00 psi (Off)       Initial pressure:  1.00 psi (Off)


                                        POST RUN
                                           Post Time: 0.00 min


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
        Sample Washes                 0
        Sample Pumps                  0
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        Nanoliter Adapter           Off
        PostInj Solvent A Washes      0
        PostInj Solvent B Washes      0
        Viscosity Delay               0 seconds
        Plunger Speed              Fast

     Back Injector:
        Sample Washes                 0
        Sample Pumps                  0
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        Nanoliter Adapter           Off
        PostInj Solvent A Washes      0
        PostInj Solvent B Washes      0
        Viscosity Delay               0 seconds
        Plunger Speed              Fast

 Column 1 Inventory Number : 1023340
 Column 2 Inventory Number :  



                            GERSTEL MAESTRO


SYSTEM SETTINGS
   Maestro Runtime         : 52.42 min
   GC Cool Down Time       : 8.00 min
   Cryo Timeout            : 15.00 min



                               GERSTEL CIS



CRYO COOLING
   Cryo Cooling            : used

TEMPERATURE PROGRAM
   Initial Temperature     : -150 'C
   Equilibration Time      : 0.20 min
   Initial Time            : 0.20 min
   Ramp 1                 
       Rate                : 12.0 'C/s
       End Temp            : 250 'C
       Hold Time           : 5.00 min
   Ramp 2                 
       Rate                : 0.0 'C/s



                               GERSTEL TDS


TEMPERATURE PROGRAM
   Initial Temperature     : 20 'C
   Delay Time              : 0.50 min
   Initial Time            : 2.00 min
   Ramp 1                 
       Rate 1              : 120.0 'C/min
       End Temp 1          : 300 'C
       Hold Time 1         : 3.00 min
   Ramp 2                 
       Rate 2              : 0.0 'C/min

TDS SETTINGS
   Transfer Temp           : 280 'C
   StandBy Temp            : 50 'C
   Vent Time               : 2.00 min
   Desorption Mode         : Solvent Venting
   Sample Mode             : StandBy Cooling

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : dftpp.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 0.00 min

EM Absolute              : False
EM Offset                : 0
Resulting EM Voltage     : 1776.5

[Scan Parameters]

Low Mass                 : 29.0
High Mass                : 500.0
Threshold                : 500
Sample #                 : 2       A/D Samples    4

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US82330258
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      17.056
 IONFOCUS    :      61.686
 ENTRANCE_LE :       0.000
 EMVOLTS     :    1776.471
 AMUGAIN     :    2223.000
 AMUOFFSET   :     127.000
 FILAMENT    :       1.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :     11.545@  3    11.545@ 50    10.290@ 69     9.537@131    10.541@219    10.541@414    10.792@502    10.792@799 
 MASSGAIN    :      14.000   
 MASSOFFSET  :     -11.000   


                           END OF TUNE PARAMETERS
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                                  END OF INSTRUMENT CONTROL PARAMETERS
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